Metrohm 757 VA Computrace Manual de usuario Pagina 95
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- SOLUCIÓN DE PROBLEMAS
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Valorado. / 5. Basado en revisión del cliente
5.2 Working method specifications
757 VA Computrace – Software
85
Documentation
In the
Documentation
tab of the
EDIT WORKING METHOD
PARAMETERS
window the elements for the automatic documenta-
tion printout at the end of the determination are defined. These
settings belong to the method and are stored with it.
Results
Automatic printout of
Full report
or
Short report
.
Font size
Font size in points for report printout.
Comment
Automatic printout of the method comment de-
fined in the accompanying field.
Determination curves
Automatic printout of all voltammograms.
Calibration
Automatic printout of all calibration curves.
Curves on two pages
If this option is checked, the determination and
calibration curves are printed on two separate
pages; if not, they are printed on one page.
- 757 VA Computrace 1
- Table of contents 3
- Exploratory mode 5
- Determination mode 6
- Troubleshooting 9
- Software license 10
- 1 Introduction 11
- 1.2 General information 12
- 1.3 Installation 13
- Method 2 16
- 1.5 Overview of file types 20
- 1.6 Context sensitive menus 20
- 2 Main window 21
- 2.3 File menu 24
- 2.4 Mode menu 26
- 2.5 Utility menu 27
- 2.6 User menu 27
- 2.7 Settings menu 31
- 2.8 Window menu 35
- 3 General settings for 37
- Voltage step 38
- Drop size 38
- [ 1...9 ; 4 ] 38
- Stirrer/RDE (rpm) 40
- [ 0...3000 rpm ; 2000 rpm ] 40
- 3.2 VA measurement modes 41
- SqW - Square wave 43
- EXPLORATORY SPECIFICATION 43
- WORKING 43
- METHOD SPECIFICATIONS 43
- DC - Sampled direct current 45
- WORKING METHOD SPECIFICATIONS 45
- NP - Normal pulse 47
- CV - Cyclic voltammetry 49
- Potential limit (V) 52
- [ -5...+5 V ; -0.1 V ] 52
- Maximum time (s) 52
- [ > 0 ; 20 s ] 52
- 3.3 Potentiostat 55
- 3.5 Graphical settings 59
- Width [ 0...8 ; 0 ] 64
- 4 Exploratory mode 65
- 4.3 Exploratory curves 70
- 5 Determination mode 81
- Voltammetric 87
- WORKING METHOD SPECIFI 87
- 5.3 Monitor 98
- <Next> 99
- 757 VA Computrace – Software 100
- 5.4 Determination curves 104
- DETERMINATION CURVES 105
- TERMINATION CURVES 105
- 5.5 Results 113
- Substances 115
- Cell volume 115
- Substance 115
- 5.6 Sample table 118
- Determination method 122
- Working method 122
- Order [ 1...6 ; ] 122
- Sample table 122
- BASELINE 126
- Front end 126
- Rear end 126
- Peak voltage 127
- Peak height 127
- Derivative 127
- Peak area 127
- CALCULATION 130
- No. of replications 132
- 6 Manual control 135
- 6.2 Dosimat control 137
- 6.3 Film deposition 138
- 6.4 Cleaning procedure 140
- 6 Manual control 142
- 7 How to ...? 143
- 7.2 User rights 144
- Measure blank 150
- No. of blanks 150
- Blank purge time 150
- <OK> 150
- 7.5 Determinations 151
- 7.9 Diagnostic procedures 166
- END OF DETERMINA 170
- 8 Troubleshooting 171
- 8.3 Software problems 172
- 8.4 Dosimat problems 172
- 8.6 Voltammetric problems 177
- Deposition time 181
- Deposition potential 181
- Exponential 187
- 8 Troubleshooting 190
- Index 193
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