Metrohm 757 VA Computrace Manual de usuario Pagina 166

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7 How to ...?
757 VA Computrace – Software
156
7.9 Diagnostic procedures
Check the purging
1. Connect the inert gas to the 757 VA Computrace Stand (see
Hardware Manual).
2. Make sure that the inert gas pressure is 1 ± 0.2 bar.
3. Add 20 mL ultrapure water to the empty measuring vessel at
the 757 VA Computrace Stand.
4. Click on or
MAIN WINDOW
/ Utility / Computrace control
to
open the
COMPUTRACE CONTROL
window.
5. Select
HMDE
and click on .
6. Make sure that inert gas bubbles are purging through the so-
lution.
Check the stirring
1. Click on or
MAIN WINDOW
/ Utility / Computrace control
to
open the
COMPUTRACE CONTROL
window.
2. Select
HMDE
and click on .
3. Change the rotational speed by clicking on the buttons of
the
RDE/stirrer speed
field.
Check the MME
1. Install the MME at the 757 VA Computrace Stand (see Hard-
ware Manual).
2. Make sure that the inert gas pressure is 1 ± 0.2 bar.
3. Add 10 mL ultrapure water to the empty measuring vessel at
the 757 VA Computrace Stand.
4. Add 0.25 mL potassium chloride c(KCl) = 1 g/L (Metrohm
No. 6.2308.020) to the measuring vessel.
5. Click on or
MAIN WINDOW
/ Utility / Computrace control
to
open the
COMPUTRACE CONTROL
window.
6. Select
DME
and click on .
7. Mercury flows out of the capillary. The typical natural drop
time is in the range of 1 - 5 sec. If the natural drop time is
smaller than 0.5 sec, change the capillary and/or needle at
the MME (see Hardware Manual).
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