Metrohm 757 VA Computrace Manual de usuario Pagina 137
- Pagina / 198
- Tabla de contenidos
- SOLUCIÓN DE PROBLEMAS
- MARCADORES
Valorado. / 5. Basado en revisión del cliente
6.2 Dosimat control
757 VA Computrace – Software
127
6.2 Dosimat control
Dosimat control selection
MAIN WINDOW
/ Utility / Dosimat control
Start manual control of the 665 or 765 Dosimats
connected to the 757 VA Computrace Stand.
Dosimat control window
The
DOSIMAT CONTROL
window serves for manual control of the
Dosimats connected to the 757 VA Computrace Stand.
Burette
Selection of the Dosimat to be controlled manu-
ally.
Switch on dosing by Dosimat. The solution is
dispensed until the
<Dose off>
button is pressed.
The burette cylinder of the Dosimat is filled.
The burette cylinder of the Dosimat is emptied
and refilled.
Dose the set
Volume
.
Volume (mL) [ > 0.01 mL ; 0 mL ]
Volume to be dosed.
Status [ read only ]
Display of the current Dosimat status.
- 757 VA Computrace 1
- Table of contents 3
- Exploratory mode 5
- Determination mode 6
- Troubleshooting 9
- Software license 10
- 1 Introduction 11
- 1.2 General information 12
- 1.3 Installation 13
- Method 2 16
- 1.5 Overview of file types 20
- 1.6 Context sensitive menus 20
- 2 Main window 21
- 2.3 File menu 24
- 2.4 Mode menu 26
- 2.5 Utility menu 27
- 2.6 User menu 27
- 2.7 Settings menu 31
- 2.8 Window menu 35
- 3 General settings for 37
- Voltage step 38
- Drop size 38
- [ 1...9 ; 4 ] 38
- Stirrer/RDE (rpm) 40
- [ 0...3000 rpm ; 2000 rpm ] 40
- 3.2 VA measurement modes 41
- SqW - Square wave 43
- EXPLORATORY SPECIFICATION 43
- WORKING 43
- METHOD SPECIFICATIONS 43
- DC - Sampled direct current 45
- WORKING METHOD SPECIFICATIONS 45
- NP - Normal pulse 47
- CV - Cyclic voltammetry 49
- Potential limit (V) 52
- [ -5...+5 V ; -0.1 V ] 52
- Maximum time (s) 52
- [ > 0 ; 20 s ] 52
- 3.3 Potentiostat 55
- 3.5 Graphical settings 59
- Width [ 0...8 ; 0 ] 64
- 4 Exploratory mode 65
- 4.3 Exploratory curves 70
- 5 Determination mode 81
- Voltammetric 87
- WORKING METHOD SPECIFI 87
- 5.3 Monitor 98
- <Next> 99
- 757 VA Computrace – Software 100
- 5.4 Determination curves 104
- DETERMINATION CURVES 105
- TERMINATION CURVES 105
- 5.5 Results 113
- Substances 115
- Cell volume 115
- Substance 115
- 5.6 Sample table 118
- Determination method 122
- Working method 122
- Order [ 1...6 ; ] 122
- Sample table 122
- BASELINE 126
- Front end 126
- Rear end 126
- Peak voltage 127
- Peak height 127
- Derivative 127
- Peak area 127
- CALCULATION 130
- No. of replications 132
- 6 Manual control 135
- 6.2 Dosimat control 137
- 6.3 Film deposition 138
- 6.4 Cleaning procedure 140
- 6 Manual control 142
- 7 How to ...? 143
- 7.2 User rights 144
- Measure blank 150
- No. of blanks 150
- Blank purge time 150
- <OK> 150
- 7.5 Determinations 151
- 7.9 Diagnostic procedures 166
- END OF DETERMINA 170
- 8 Troubleshooting 171
- 8.3 Software problems 172
- 8.4 Dosimat problems 172
- 8.6 Voltammetric problems 177
- Deposition time 181
- Deposition potential 181
- Exponential 187
- 8 Troubleshooting 190
- Index 193
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